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Does file size make difference? Do smaller files get to the network drive but larger files are failing?
It could also be a network latency issue where MathCAD is overwriting the network transfer speed and the server is saying 'I'm full'.
What does your IT department say about it?
Verify Path Length: If the file or directory path exceeds 260 characters, Windows may prevent saving data. Consider shortening folder or file names to avoid this limitation. if it is Map the long pathname to a drive like Z: or similar.